General Directions for Calibration
المؤلف:
D. A. Skoog, F. J.Holler, D M. West, and S. R. Crouch
المصدر:
Fundamentals of Analytical Chemistry
الجزء والصفحة:
9th ed - p43
8-8-2016
1116
General Directions for Calibration
All volumetric ware should be painstakingly freed of water breaks before being calibrated. Burets and pipets need not be dry, but volumetric flasks should be thoroughly drained and dried at room temperature. The water used for calibration should be in thermal equilibrium with its surroundings. This condition is best established by drawing the water well in advance, noting its temperature at frequent intervals, and waiting until no further changes occur.
Although an analytical balance can be used for calibration, weighings to the nearest milligram are perfectly satisfactory for all but the very smallest volumes. Thus, a toploading balance is more convenient to use than an analytical balance. Weighing bottles or small, well-stoppered conical flasks can serve as receivers for the calibration liquid.
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